HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86643533, compound → (3-Aminophenyl)methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86643533 | HCID 86643533 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (3-Aminophenyl)methanesulfonamide | HCID 13266255 | 95% |
Reaction Steps
(3-Nitrophenyl)methanesulfonyl amide (3.5 g, 16 mM) was hydrogenated over Raney-Ni (0.5 g) in methanol at 50° C. and 70 psi for 4 hours. Then the catalyst was filtered off and washed with warm methanol. The combined filtrates were evaporated to give 2.83 g (95%) of (3-amino-phenyl)-methanesulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436007B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-30eace4a6bf24578a0f9337792d5d3b4 |
| Source note | uspto-grants-2013_05 |