反应详情

A mixture of 4-bromo-2-chloropyridine (0.5 g, 2.6 mmol) and cyclohexylamine (0.26 g, 2.6 mmol) was heated in a CEM Microwave at 150 degrees for 15 minutes at 300 W. The resulting crude material was purified by flash chromatography (0% to 30% ethyl acetate/hexane) to give 85 mg of the title compound. MS m/z 256.8 (ESI: M+H)+.

1. temperaturewas heated in a CEM Microwave at 150 degrees for 15 minutes at 300 W
2. customThe resulting crude material was purified by flash chromatography (0% to 30% ethyl acetate/hexane)