HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → Trifluoroacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 87191588 | HCID 87191588 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 87192459 | HCID 87192459 | — |
Reaction Steps
A solution of Example 261b (1.76 g, 2.88 mmol) in CH2Cl2 (30 mL) was treated with trifluoroacetic acid (3.32 mL, 43.1 mmol). The mixture is stirred at room temperature for 3 hours and concentrated to give 2.34 of the title compound as trifluoroacetic acid salts.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435980B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-15a2ae01ec7141ed8852f23f14730133 |
| Source note | uspto-grants-2013_05 |