Triethylamine → HCID 87192197, compound

Participants

Reaction Steps

A mixture of Example 42b (1 g, 2.23 mmol), cyclohexane-1,3-diamine (0.509 g, 4.46 mmol) and triethylamine (0.62 mL, 4.46 mmol) in dioxane (25 mL) was heated at 60° C. for 2 hours. The reaction mixture was concentrated and used directly for the next step.

Provenance & Evidence