HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178511663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 87192404 | HCID 87192404 | — |
| Reactant | HCID 178511674 | HCID 178511674 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178511663 | HCID 178511663 | — |
Reaction Steps
A mixture of Example 42b (5 g, 11.14 mmol), trans-cyclohexane-1,4-diamine (2.54 g, 22.28 mmol), triethylamine (3.10 mL, 22.28 mmol) and dioxane (120 mL) in a 250 mL of flask was heated at 60° C. for 90 minutes. The reaction mixture was concentrated and used directly for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435980B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-6ffddaa1a7b4443ca3a14594bc3a12ac |
| Source note | uspto-grants-2013_05 |