反应详情

The reaction is diluted with water and extracted with dichloromethane. After drying (Na2SO4) the solvent is removed to give an oil. The product is purified by chromatography (silica, ethyl acetate/hexane) to give a geometrical mixture of isomers containing 2-Methyl-1,2,6,7,8,9-hexahydro-cyclopenta[.a.]naphthalen-3-one and the title compound.

1. extractionextracted with dichloromethane
2. dry with materialAfter drying (Na2SO4) the solvent
3. customis removed
4. customto give an oil
5. customThe product is purified by chromatography (silica, ethyl acetate/hexane)
6. customto give
7. additiona geometrical mixture of isomers
8. additioncontaining 2-Methyl-1,2,6,7,8,9-hexahydro-cyclopenta[.a