HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-methyl-2,3,5,6,7,8-hexahydro-1H-cyclopenta[b]naphthalen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Naphthalen-3-one | HCID 20192716 | — |
| Product | 2-methyl-2,3,5,6,7,8-hexahydro-1H-cyclopenta[b]naphthalen-1-one | HCID 22499222 | — |
Reaction Steps
The reaction is diluted with water and extracted with dichloromethane. After drying (Na2SO4) the solvent is removed to give an oil. The product is purified by chromatography (silica, ethyl acetate/hexane) to give a geometrical mixture of isomers containing 2-Methyl-1,2,6,7,8,9-hexahydro-cyclopenta[.a.]naphthalen-3-one and the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436017B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-f6363a541244451d9f99629d4227ec76 |
| Source note | uspto-grants-2013_05 |