HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(5-Ethyl-2-methyl-indan-2-yl)-benzamide → N-(5-Ethyl-2-methyl-indan-2-yl)-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(5-Ethyl-2-methyl-indan-2-yl)-benzamide | HCID 22499186 | — |
| Reactant | N-(5-acetyl-2-methyl-indan-2-yl)-benzamide | HCID 22499217 | — |
| Product | N-(5-Ethyl-2-methyl-indan-2-yl)-benzamide | HCID 22499186 | — |
| Product | N-(5-Acetyl-6-ethyl-2-methyl-indan-2-yl)-benzamide | HCID 22499225 | — |
Reaction Steps
N-(5-Acetyl-6-ethyl-2-methyl-indan-2-yl)-benzamide is prepared from N-(5-ethyl-2-methyl-indan-2-yl)-benzamide (2.6 g) following the procedure used to prepare N-(5-acetyl-2-methyl-indan-2-yl)-benzamide. The product is purified by chromatography (silica, hexane/ethyl acetate, 4:1) to give the title compound. ES+ MS m/e 322 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436017B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-e737796fb3774b369686176398e34617 |
| Source note | uspto-grants-2013_05 |