HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → 1-(1-methyl-4-nitro-1H-pyrazol-5-yl)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-chloro-1-methyl-4-nitro-1H-pyrazole | HCID 12344836 | — |
| Product | 1-(1-methyl-4-nitro-1H-pyrazol-5-yl)piperidine | HCID 3413119 | 89% |
Reaction Steps
Reaction of 5-chloro-1-methyl-4-nitro-1H-pyrazole and piperidine gave 1-(1-methyl-4-nitro-1H-pyrazol-5-yl)piperidine as a white solid (232 mg, 89%). 1H NMR (400 MHz, CDCl3) δ 8.00 (s, 1H), 3.74 (s, 3H), 3.18-3.12 (m, 4H), 1.74-1.63 (m, 6H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436001B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-ee51aa8e9a664edf9e4e04751073e4ff |
| Source note | uspto-grants-2013_05 |