Iodine → HCID 178526522, compound

Participants

Reaction Steps

7-Nitroindazole (1.60 g, 9.80 mmol) was dissolved in DMF (100 mL), and potassium hydroxide (2.20 g, 39.20 mmol) and iodine (4.98 g, 19.61 mmol) were added in drops thereto. After stirring for 2 h, the reaction mixture was diluted with 10% aqueous sodium bisulfate solution. The resulting solid was collected and dried to give the title compound (2.50 g, Yield 88%).

Provenance & Evidence