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HRID2090113

反应详情

EQUATION

反应方程式

HRID 2090113 的结构方程式

REACTANTS

反应物

2
结构：C=C(C)CC(C)(C)C
HCID7868

2,4,4-Trimethyl-1-pentene

C8H16

结构：O=[PH2]O
HCID4124402

Phosphinic acid

H3O2P

PRODUCTS

生成物

1
结构：CC(C[PH](=O)O)CC(C)(C)C
HCID178460681

未命名化合物

PROCEDURE

实验过程

A mixture of diisobutylene (112 g, 1 mol) and hypophosphorous acid (30%, 230 mL) are reacted in the presence of t-butyfperbenzoate. After aqueous work up, 45 g of oily product are obtained. It is characterized by 1H NMR and 31P NMR which shows formation of product (64% pure).

WORKUP

后处理

  1. customare reacted in the presence of t-butyfperbenzoate