HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,4-Trimethyl-1-pentene → HCID 178460681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,4-Trimethyl-1-pentene | HCID 7868 | — |
| Reactant | Phosphinic Acid | HCID 4124402 | — |
| Product | HCID 178460681 | HCID 178460681 | — |
Reaction Steps
A mixture of diisobutylene (112 g, 1 mol) and hypophosphorous acid (30%, 230 mL) are reacted in the presence of t-butyfperbenzoate. After aqueous work up, 45 g of oily product are obtained. It is characterized by 1H NMR and 31P NMR which shows formation of product (64% pure).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436131B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-d70112fb6db740aa9d9a0bdf25086428 |
| Source note | uspto-grants-2013_05 |