HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 25106689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 68432292 | HCID 68432292 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 25106689 | HCID 25106689 | — |
Reaction Steps
The product from step (vi) (30 mg) was dissolved in DMF (2 mL) then a solution of dimethylamine (2M in THF, 0.279 mL) was added at rt under nitrogen. The resulting solution was stirred at rt for 16 h. The mixture was purified by RPHPLC to give the title compound, yield 4.5 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436178B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-fce58ec914cd4d119d2ac232c5bdee8a |
| Source note | uspto-grants-2013_05 |