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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2090250Generated: November 1, 2026

Methanol → HCID 25106691, compound

https://huagongshe.com/reaction/2090250

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSulfuric AcidHCID 1118—
ReactantHCID 68431610HCID 68431610—
ProductHCID 25106691HCID 25106691—

Reaction Steps

Sulfuric acid (1 mL) was added to the product from step (i) (250 mg) in MeOH (10 mL). The mixture was stirred at rt for 15 h, then the solvent evaporated under reduced pressure. The residue was purified by RPHPLC to afford the title compound, yield 6.2 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08436178B2
Source datasetuspto-grants-2013_05
ORD IDord-972886bb661a48428f3f5ca71c52adaa
Source noteuspto-grants-2013_05