HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 25106691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 68431610 | HCID 68431610 | — |
| Product | HCID 25106691 | HCID 25106691 | — |
Reaction Steps
Sulfuric acid (1 mL) was added to the product from step (i) (250 mg) in MeOH (10 mL). The mixture was stirred at rt for 15 h, then the solvent evaporated under reduced pressure. The residue was purified by RPHPLC to afford the title compound, yield 6.2 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436178B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-972886bb661a48428f3f5ca71c52adaa |
| Source note | uspto-grants-2013_05 |