HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11033857, compound → Ethyl 3-oxododecanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11033857 | HCID 11033857 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-oxododecanoate | HCID 3017756 | 98% |
Reaction Steps
The resulting 5-decanoyl-2,2-dimethyl-1,3-dioxane-4,6-dione was allowed to reflux in ethanol for 2 hours, and then concentrated under reduced pressure. The resulting residue was purified using silica gel chromatography (developing solvent: n-hexane/ethyl acetate=3/7) to obtain the ethyl 3-oxododecanoate shown by the formula below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436210B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-7c9fd7c3503b41568ac8030551dd972c |
| Source note | uspto-grants-2013_05 |