HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Acetyltetralin → 2-Bromo-1-(5,6,7,8-tetrahydronaphthalen-2-yl)ethan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Acetyltetralin | HCID 69885 | — |
| Reactant | Phenyltrimethylammonium bromide dibromide | HCID 17977687 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Bromo-1-(5,6,7,8-tetrahydronaphthalen-2-yl)ethan-1-one | HCID 7353991 | — |
Reaction Steps
25 g (143 mmol) of 1-(5,6,7,8-tetrahydronaphthalen-2-yl)ethanone are dissolved in 750 ml of THF, 64.7 g (172 mmol) of phenyltrimethylammonium tribromide are added, and the mixture is stirred at room temperature for 15 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436186B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-52019c7f0fde4a39bdb69c5d85775165 |
| Source note | uspto-grants-2013_05 |