HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 66778180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | Methyl 4-methoxyacetoacetate | HCID 123500 | — |
| Reactant | 4-Methoxyphenylhydrazine hydrochloride | HCID 2723904 | — |
| Product | HCID 66778180 | HCID 66778180 | 50% |
Reaction Steps
Using methyl 4-methoxyacetoacetate (5.8 g), dimethylformamide dimethylacetal (5.4 mL) and 4-methoxyphenylhydrazine hydrochloride (7.0 g) and in the same manner as in Example 15(1), the title object compound (5.5 g, 50%) was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436043B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-994fb35e9d66404bba1a2df70f95c034 |
| Source note | uspto-grants-2013_05 |