HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine hydrochloride → HCID 66777473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine hydrochloride | HCID 60962 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | Methyl 4-methoxyacetoacetate | HCID 123500 | — |
| Product | HCID 66777473 | HCID 66777473 | 55% |
Reaction Steps
Using methyl 4-methoxyacetoacetate (7.9 g), dimethylformamide dimethylacetal (7.2 mL) and phenylhydrazine hydrochloride (5.8 g) and in the same manner as in Example 15(1), the title object compound (7.3 g, 55%) was obtained as a pale-yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436043B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-c251c6b632df4a2dbd86795abdb6afe0 |
| Source note | uspto-grants-2013_05 |