反应详情

To bicyclo[3.3.1]non-6-en-3-amine (100 mg, 0.729 mmol) in ethanol (3 mL), 10% palladium-carbon (10 mg) was added in a nitrogen stream, and the reaction solution was stirred in a hydrogen stream at room temperature for 1 day. After completion of the reaction, the reaction solution was filtered through celite and the filtrate was evaporated under reduced pressure. The resulting crude reaction product was used for the next step without to further purification (98.5 mg).

1. customAfter completion of the reaction
2. filtrationthe reaction solution was filtered through celite
3. customthe filtrate was evaporated under reduced pressure
4. customThe resulting crude reaction product
5. customwas used for the next step without to further purification (98.5 mg)