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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2092050Generated: October 31, 2026

bicyclo[3.3.1]non-6-en-3-amine → HCID 21522752, compound

https://huagongshe.com/reaction/2092050

Reaction equation

Participants

RoleNameHCIDCharge
Reactantbicyclo[3.3.1]non-6-en-3-amineHCID 424483—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 21522752HCID 21522752—

Reaction Steps

To bicyclo[3.3.1]non-6-en-3-amine (100 mg, 0.729 mmol) in ethanol (3 mL), 10% palladium-carbon (10 mg) was added in a nitrogen stream, and the reaction solution was stirred in a hydrogen stream at room temperature for 1 day. After completion of the reaction, the reaction solution was filtered through celite and the filtrate was evaporated under reduced pressure. The resulting crude reaction product was used for the next step without to further purification (98.5 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08440666B2
Source datasetuspto-grants-2013_05
ORD IDord-f784df98c5134ac89cb941fe2a3c653a
Source noteuspto-grants-2013_05