HuagongsheHuagongshe Chemistry Print Report · For research reference only
bicyclo[3.3.1]non-6-en-3-amine → HCID 21522752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | bicyclo[3.3.1]non-6-en-3-amine | HCID 424483 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21522752 | HCID 21522752 | — |
Reaction Steps
To bicyclo[3.3.1]non-6-en-3-amine (100 mg, 0.729 mmol) in ethanol (3 mL), 10% palladium-carbon (10 mg) was added in a nitrogen stream, and the reaction solution was stirred in a hydrogen stream at room temperature for 1 day. After completion of the reaction, the reaction solution was filtered through celite and the filtrate was evaporated under reduced pressure. The resulting crude reaction product was used for the next step without to further purification (98.5 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440666B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-f784df98c5134ac89cb941fe2a3c653a |
| Source note | uspto-grants-2013_05 |