HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59574324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Mucobromic Acid | HCID 3033972 | — |
| Reactant | 2-((Pyridin-4-yl)methyl)hydrazine hydrochloride | HCID 22728080 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59574324 | HCID 59574324 | 59% |
Reaction Steps
4-Picolylhydrazine hydrochloride (500 mg, 3.13 mmol), mucobromic acid (807 mg, 3.13 mmol) and concentrated hydrochloric acid (500 μL) in ethanol (5 mL) were stirred at 90° C. for 1 day. After completion of the reaction, the resulting crystals were collected by filtration, washed with methanol and dried to give the desired product (59% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440666B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-b9305bb9f1a64a73a42c22ac451b4985 |
| Source note | uspto-grants-2013_05 |