HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 68429239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 59574457 | HCID 59574457 | — |
| Product | HCID 68429239 | HCID 68429239 | 51% |
Reaction Steps
2-[5-Bromo-4-{[5-(methoxymethoxy)tricyclo[3.3.1.13,7]dec-2-yl]amino}-6-oxopyridazin-1(6H)-yl]-N-(pyridin-4-ylmethyl)acetamide (30 mg, 0.0563 mmol) in 10 mass % hydrogen chloride-methanol (3 mL) was stirred at room temperature for 1 hour. After completion of the reaction, the reaction solution was evaporated under reduced pressure, and the resulting solid was collected by filtration and dried to give the desired product (51% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440666B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-75835a35b1074c7e975165d1b7455dd9 |
| Source note | uspto-grants-2013_05 |