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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2092121Generated: October 31, 2026

Hydrochloride methanol → HCID 68429239, compound

https://huagongshe.com/reaction/2092121

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloride methanolHCID 21893726—
ReactantHCID 59574457HCID 59574457—
ProductHCID 68429239HCID 6842923951%

Reaction Steps

2-[5-Bromo-4-{[5-(methoxymethoxy)tricyclo[3.3.1.13,7]dec-2-yl]amino}-6-oxopyridazin-1(6H)-yl]-N-(pyridin-4-ylmethyl)acetamide (30 mg, 0.0563 mmol) in 10 mass % hydrogen chloride-methanol (3 mL) was stirred at room temperature for 1 hour. After completion of the reaction, the reaction solution was evaporated under reduced pressure, and the resulting solid was collected by filtration and dried to give the desired product (51% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08440666B2
Source datasetuspto-grants-2013_05
ORD IDord-75835a35b1074c7e975165d1b7455dd9
Source noteuspto-grants-2013_05