HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59393690, compound → HCID 59393695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59393690 | HCID 59393690 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 59393695 | HCID 59393695 | — |
Reaction Steps
A solution of 1b (0.896 mmol) in xylene (6.00 mL) was heated to 110° C. for approximately 1 h. After cooling to rt, the reaction mixture was concentrated in vacuo to afford the title compound 1c, which was used without further purification in the subsequent reaction. m/z (ES) 473 (MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440672B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-f5e9d3a56c9e4af2b3956c16d97a0c98 |
| Source note | uspto-grants-2013_05 |