HCID 67236455, compound → HCID 11638123, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure as described in Example 1E, substituting the product of Example 16C for the product of Example 1D. 1H NMR (300 MHz, DMSO-d6) δ 13.00 (broad s, 1H), 8.58 (s, 1H), 8.03 (s, 1H), 7.65 (d, J=7.5 Hz, 1H), 7.30 (d, J=7.5 Hz, 1H), 7.20 (m, 2H), 7.05 (d, J=6 Hz, 1H), 6.95-6.80 (m, 3H), 4.90 (m, 1H), 4.30-4.17 (m, 2H), 2.20-2.00 (m, 2H). MS (DCI) m/e 309 (M+H)+. Calcd. For C17H16N4O2.0.6; H2O: C, 63.98; H, 5.43; N, 17.56. Found: C, 63.85; H, 5.07; N, 17.62.

Provenance & Evidence