HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → Ethyl 2-(3-bromo-4-fluorophenyl)acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 3-Bromo-4-fluorophenylacetic Acid | HCID 3416339 | — |
| Produkt | Ethyl 2-(3-bromo-4-fluorophenyl)acetate | HCID 58539475 | — |
Reaktionsschritte
3-Bromo-4-fluorophenylacetic acid (2.35 g, 9.0 mmol) was treated with concentrated sulfuric acid (2 mL) in ethanol (100 mL) at reflux for 2 hours. Purification by silica gel chromatography provided the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08440707B2 |
| Quelldatensatz | uspto-grants-2013_05 |
| ORD ID | ord-c27a18d723cd4e3aa4a3be4aa1d94693 |
| Quellennotiz | uspto-grants-2013_05 |