N-methylhydroxylamine hydrochloride → HCID 24959566, compound

Participants

Reaction Steps

Following the same procedure described for 4 and starting from 2 (1.6 mmol) and N-methylhydroxylamine hydrochloride (2 mmol), after workup compound 5 was isolated as a colourless oil (0.34 g, yield 63%). [α]D=+10.5 (c=0.5; CH3OH). 1H-NMR (CDCl3) δ 7.65 (d, 2H, J=7 Hz), 7.30 (d, 2H, J=7 Hz), 2.90 (s, 3H), 1.94 (d, 3H, J=23 Hz).

Provenance & Evidence