Hydrochloric Acid → HCID 51038883, compound

Participants

Reaction Steps

To 7C (30 mg, 0.10 mmol) in 2 mL of 1,4-dioxane was added HCl (4N in 1,4-dioxane, 1.0 mL). The mixture was stirred at rt for overnight. The solvent was removed under vacuum. The resulting residue was dissolved in 2 mL of water and was washed with EtOAc (5 mL×3). The water was the removed under vacuum to give the title compound as hydrogen chloride salts (7) respectively (20 mg). LC-MS (ESR): m/z=177 (M+H)+

Provenance & Evidence