HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 51038898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 67054470 | HCID 67054470 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 51038898 | HCID 51038898 | — |
Reaction Steps
To 16A (30 mg, 0.10 mmol) in was added HBr (30% in HOAc) 1 mL and the mixture was stirred at rt for 2 h. Ether (10 mL×2) was added and the resulting precipitate was collected and dried under vacuum to give the title compound as hydrogen bromide salts (16). LC-MS (ESR): m/z=196 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440720B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-7942e5bb4a784194871b156774f1bca2 |
| Source note | uspto-grants-2013_05 |