4-Ethylphenethylamine → HCID 52911978, compound

HRID 2092685Notes

Reaction equation

C(O[C:4]([C:6]1([CH2:13][CH2:14]OC)[CH2:11][CH2:10][CH:9]([OH:12])[CH2:8][CH2:7]1)=[O:5])C.[CH2:17]([C:19]1[CH:24]=[CH:23][C:22]([CH2:25][CH2:26][NH2:27])=[CH:21][CH:20]=1)[CH3:18]>>[CH2:17]([C:19]1[CH:24]=[CH:23][C:22]([CH2:25][CH2:26][N:27]2[CH2:14][CH2:13][C:6]3([CH2:7][CH2:8][CH:9]([OH:12])[CH2:10][CH2:11]3)[C:4]2=[O:5])=[CH:21][CH:20]=1)[CH3:18]

Participants

Reactant 2

HCID 1440474-Ethylphenethylamine

HCID 582299764-Hydroxy-1-(2-methoxy-ethyl)-cyclohexanecarboxylic acid ethyl ester

Product 1

HCID 52911978HCID 52911978, compound

Procedure

The title compound was prepared in analogy to example 1, step 4 from 4-hydroxy-1-(2-methoxy-ethyl)-cyclohexanecarboxylic acid ethyl ester (obtained in example 2, step 3) by treatment with 2-(4-ethylphenyl)-ethylamine [CAS Reg. No. 64353-29-3]. MS (m/e): 302.3 [MH+].

Sources & evidence

ORD record: ord-dc6511f38bb143fe894678b4f730d6b3
Source dataset: uspto-grants-2013_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08440710B2

Reaction notes

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