HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58230115, compound → HCID 66579360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58230115 | HCID 58230115 | — |
| Solvent | Diethylether heptane | HCID 21897273 | — |
| Product | HCID 66579360 | HCID 66579360 | — |
Reaction Steps
This material was obtained in analogy to example 108, step 4 by Swern oxidation of 8-hydroxy-2-[4-(2,2,2-trifluoro-1-methyl-ethoxy)-phenyl]-2-aza-spiro[4.5]decan-1-one (230 mg, obtained in example 162, step 3) as a colorless solid (230 mg). Rf: 0.3 (silica gel, ether/heptane 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440710B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-03b123ce6ea24c3c90991cf865f2bb6a |
| Source note | uspto-grants-2013_05 |