HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic acid 4-amino-phenyl ester → HCID 58230095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic acid 4-amino-phenyl ester | HCID 19885019 | — |
| Reactant | 4-Hydroxy-1-(2-methoxy-ethyl)-cyclohexanecarboxylic acid ethyl ester | HCID 58229976 | — |
| Product | HCID 58230095 | HCID 58230095 | — |
Reaction Steps
The title compound was prepared in analogy to example 108, step 3 from 4-hydroxy-1-(2-methoxy-ethyl)-cyclohexanecarboxylic acid ethyl ester (obtained in example 2, step 3) by treatment with methanesulfonic acid 4-amino-phenyl ester (synthesis: S. Kobayashi, et al.; Synlett. 2000, p 883) as a mixture of cis and trans diastereomers. MS (m/e): 340.121 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440710B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-0b3af366129341d1bef91d32a180427f |
| Source note | uspto-grants-2013_05 |