HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-4-tert-butylbenzene → 10-(4-tert-Butyl-phenyl)-1,4-dioxa-10-aza-dispiro[4.2.4.2]tetradecan-9-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-4-tert-butylbenzene | HCID 77595 | — |
| Reactant | 1,4-Dioxa-10-azadispiro[4.2.4.2]tetradecan-9-one | HCID 58230108 | — |
| Product | 10-(4-tert-Butyl-phenyl)-1,4-dioxa-10-aza-dispiro[4.2.4.2]tetradecan-9-one | HCID 66579508 | — |
Reaction Steps
The title compound was prepared in analogy to example 336, step 1 from 1,4-dioxa-10-aza-dispiro[4.2.4.2]tetradecan-9-one (described in example 133, step 3) and 1-bromo-4-tert-butyl-benzene. White solid (84%). MS (m/e): 344.2 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440710B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-51e669bc5a7b4ac0882d3609b92feeae |
| Source note | uspto-grants-2013_05 |