Hydrochloric Acid → HCID 66579407, compound

HRID 2092710Notes

Reaction equation

HRID 2092710 reaction equation
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([N:11]2[CH2:24][CH2:23][C:13]3([CH2:22][CH2:21][C:16]4(OCC[O:17]4)[CH2:15][CH2:14]3)[C:12]2=[O:25])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].Cl>>[C:1]([C:5]1[CH:6]=[CH:7][C:8]([N:11]2[CH2:24][CH2:23][C:13]3([CH2:22][CH2:21][C:16](=[O:17])[CH2:15][CH2:14]3)[C:12]2=[O:25])=[CH:9][CH:10]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 6657950810-(4-tert-Butyl-phenyl)-1,4-dioxa-10-aza-dispiro[4.2.4.2]tetradecan-9-one

Product 1

HCID 66579407HCID 66579407, compound

Procedure

The title compound was prepared in analogy to example 133 step 5 from 10-(4-tert-butyl-phenyl)-1,4-dioxa-10-aza-dispiro[4.2.4.2]tetradecan-9-one (described in example 343, step 1) by treatment with 2M HCl. Off-white solid (90%). MS (m/e): 300.4 [MH+].

Sources & evidence

ORD record
ord-6bcab0b912fc463e9d26bca3c694f24a
Source dataset
uspto-grants-2013_05
Patent number
US08440710B2

Reaction notes

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