HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Methylsulfonyl)piperazine → HCID 44545388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Methylsulfonyl)piperazine | HCID 709161 | — |
| Reactant | HCID 58015218 | HCID 58015218 | — |
| Product | HCID 44545388 | HCID 44545388 | — |
Reaction Steps
2-(2-(2-(tert-butoxycarbonylamino)pyrimidin-5-yl)-6-morpholino-9H-purin-9-yl)acetic acid (35 mg) was reacted with 1-(methylsulfonyl)piperazine via General Procedure E followed by Boc deprotection via General Procedure D and purified via reverse phase HPLC to give 9 mg 123 as a white solid. MS (Q1) 503.2 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445487B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-086436cb94ea41048ad5c1e03d5f32f5 |
| Source note | uspto-grants-2013_05 |