HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 68726219, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Cyanuric chloride | HCID 7954 | — |
| Reactant | HCID 68724707 | HCID 68724707 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68726219 | HCID 68726219 | — |
Reaction Steps
To a solution of 4-hydroxy-3-(trifluoromethoxy)benzamide (532 mg, 2.41 mmol) in dimethylformamide (3 ml) was added cyanuric chloride (223 mg, 1.21 mmol). The mixture was stirred for 25 and then water was added and the resulting solution was extracted 3 times with ethyl acetate. The combined organics were washed with brine, dried over sodium sulfate, and concentrated in vacuo to afford the title compound. Mass spectrum (ESI) 202.1 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445480B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-aec3fb1e187749468b29b12beaa4a742 |
| Source note | uspto-grants-2013_05 |