Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 66868123 | HCID 66868123 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66867126 | HCID 66867126 | — |
Reaction Steps
4-Fluoro-3-methoxymethoxy-phenol from example A1 (6.89 g; 40.0 mmol) is dissolved in dry di-chloromethane (160.0 mL). The stirred solution is cooled to −15° C. N-bromosuccinimide (7.12 g; 40.0 mmol) is added in small portions over one hour. After complete addition the reaction mixture is stirred for another 30 min at −15° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08445501B2 |
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| Source dataset | uspto-grants-2013_05 |
|---|
| ORD ID | ord-6fd666a8587e4e4b9870f15934a74b6f |
|---|
| Source note | uspto-grants-2013_05 |
|---|
