Ethanol → HCID 67364813, compound

HRID 2094283Notes

Reaction equation

HRID 2094283 reaction equation
[O:1]=[S:2]1(=[O:20])[NH:7][CH2:6][CH2:5][CH:4](C)[N:3]1[C:9]1[CH:18]=[CH:17][C:12]([C:13]([O:15]C)=[O:14])=[CH:11][C:10]=1[CH3:19].[OH-].[Li+].[CH2:23](O)C>>[O:1]=[S:2]1(=[O:20])[N:7]([CH3:23])[CH2:6][CH2:5][CH2:4][N:3]1[C:9]1[CH:18]=[CH:17][C:12]([C:13]([OH:15])=[O:14])=[CH:11][C:10]=1[CH3:19]

Participants

4

Reactant 3

HCID 702EthanolHCID 3939Lithium HydroxideHCID 67048665HCID 67048665, compound

Product 1

HCID 67364813HCID 67364813, compound

Procedure

Prepared analogously to Example 39d from methyl 4-(1,1-dioxo-3-methyl-[1,2,6]thiadiazinan-2-yl)-3-methyl-benzoate and lithium hydroxide in ethanol.

Sources & evidence

ORD record
ord-2db9273affb4437290cc55f1566cd770
Source dataset
uspto-grants-2013_05
Patent number
US08445525B2

Reaction notes

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