Water → HCID 67367308, compound

HRID 2094303Notes

Reaction equation

HRID 2094303 reaction equation
[O:1]=[S:2]1(=[O:20])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][N:3]1[C:9]1[CH:18]=[CH:17][C:12]([C:13]([O:15]C)=[O:14])=[CH:11][C:10]=1[CH3:19].[OH-].[Li+].O>C(O)C>[O:1]=[S:2]1(=[O:20])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][N:3]1[C:9]1[CH:18]=[CH:17][C:12]([C:13]([OH:15])=[O:14])=[CH:11][C:10]=1[CH3:19]

Participants

5

Reactant 3

HCID 962WaterHCID 3939Lithium HydroxideHCID 67048761Methyl 4-(1,1-dioxo-[1,2]thiazepan-2-yl)-3-methyl-benzoate

Product 1

HCID 67367308HCID 67367308, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 39d from methyl 4-(1,1-dioxo-[1,2]thiazepan-2-yl)-3-methyl-benzoate and lithium hydroxide in a solvent mixture of water and ethanol.

Sources & evidence

ORD record
ord-a150f67a11da4dc499f443f6811f5c2f
Source dataset
uspto-grants-2013_05
Patent number
US08445525B2

Reaction notes

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