HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 49830481, compound → HCID 68515201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 49830481 | HCID 49830481 | — |
| Solvent | HCID 18509146 | HCID 18509146 | — |
| Product | HCID 68515201 | HCID 68515201 | — |
Reaction Steps
The title compounds were prepared by subjecting the compound of Example 4 to a column chromatography with a chiral stationary phase (Prep HPLC; column: Whelk O 2.5 cm ID×25 cm; mobile phase: hexane/EtOH/MeOH/DEA=50/25/25/0.1; flow rate: 40 ml/min; detector: UV 270 nm; column temp: RT; sample preparation: 10 mg/ml; load: 10 ml (100 mg))
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445686B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-3a362975e38f4a9b9f71c57d58588407 |
| Source note | uspto-grants-2013_05 |