3-Methoxybenzyl bromide → HCID 25207618, compound

Participants

Reaction Steps

Prepared as in example 5-10 from Methyl 4-(N-(4-methoxybenzyl)sulfamoyl)benzoate (Example 5-10b) and 3-methoxybenzyl bromide. MS (M−H, 440.50); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 3.58(s, 3H), 3.68(s, 3H), 4.24(s, 2H), 4.25(s, 2H), 6.50(s, 1H), 6.64(d, J=4 Hz, 1H), 6.73(m, 1H), 6.77(d, J=8 Hz, 2H), 7.00(d, J=8 Hz, 2H), 7.12(t, J=8 Hz, 1H), 7.94(d, J=8 Hz, 2H), 8.09(d, J=8 Hz, 2H), 13.49(s, 1H).

Provenance & Evidence