Salicylaldehyde → HCID 12155969, compound

HRID 2094961Notes

Reaction equation

[CH3:1][O:2][C:3](=[O:6])[CH2:4][NH2:5].[OH:7][C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH:10]=O>>[OH:7][C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH2:10][NH:5][CH2:4][C:3]([O:2][CH3:1])=[O:6]

Participants

Reactant 2

HCID 6998Salicylaldehyde

HCID 69221Glycine methyl ester

Product 1

HCID 12155969HCID 12155969, compoundYield 40%

Procedure

Prepared as in example 10-10a from glycine methyl ester and 2-hydroxybenzaldehyde. Yield 40%. MS M+H calculated 196.1; found 196.1

Sources & evidence

ORD record: ord-a49ae6ec221346fdb6a195c6732f26c9
Source dataset: uspto-grants-2013_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08445692B2

Reaction notes

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