HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 58232203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Propenoic acid, 3-(3-chlorophenyl)- | HCID 735250 | — |
| Reactant | HCID 67074641 | HCID 67074641 | — |
| Product | HCID 58232203 | HCID 58232203 | 72% |
Reaction Steps
In analogy to the procedure described in example 1, (R)-4-hydroxy-N,N-dimethyl-2-(7-oxo-[1,4]diazepan-1-yl)-butyramide hydrochloride and (E)-3-chlorocinnamic acid with 1.1 eq. of triethylamine gave the titled compound in 72% yield as white foam. MS: 408.1 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445674B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-726497e2df8d4ccfaead48f535e36581 |
| Source note | uspto-grants-2013_05 |