HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpiperidin-4-ol → HCID 58232093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpiperidin-4-ol | HCID 15649174 | — |
| Reactant | HCID 67074220 | HCID 67074220 | — |
| Product | HCID 58232093 | HCID 58232093 | 51% |
Reaction Steps
In analogy to the procedure described in Example 15, 3-[(S)-4-(3,4-dichloro-phenylcarbamoyl)-3-methyl-2-oxo-piperazin-1-yl]-propionic acid (intermediate 12) and 4-methyl-piperidin-4-ol gave the titled compound in 51% yield as off-white solid. MS: 471.2 (MH+, 2Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445674B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-ccd61bd143674574951a34eaf701d898 |
| Source note | uspto-grants-2013_05 |