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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2095813Generated: October 28, 2026

Diethyl (ethoxymethylene)malonate → HCID 58158628, compound

https://huagongshe.com/reaction/2095813

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl (ethoxymethylene)malonateHCID 6871—
ReactantPotassium CarbonateHCID 11430—
Reactant2-Chlorophenylhydrazine hydrochlorideHCID 443287—
SolventWaterHCID 962—
ProductHCID 58158628HCID 5815862878%

Reaction Steps

In the same manner as in Reference Example 63 and using (2-chlorophenyl)hydrazine•hydrochloride (5 g, 28 mmol), water (100 mL), potassium carbonate (8.5 g, 62 mmol) and diethyl ethoxymethylenemalonate (7.3 g, 34 mmol) as starting materials, the title compound (5.8 g, 78%) was obtained as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08445509B2
Source datasetuspto-grants-2013_05
ORD IDord-73c5d82c64d0478d9cbfd71b4939f4ba
Source noteuspto-grants-2013_05