HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (ethoxymethylene)malonate → HCID 58158628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chlorophenylhydrazine hydrochloride | HCID 443287 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58158628 | HCID 58158628 | 78% |
Reaction Steps
In the same manner as in Reference Example 63 and using (2-chlorophenyl)hydrazine•hydrochloride (5 g, 28 mmol), water (100 mL), potassium carbonate (8.5 g, 62 mmol) and diethyl ethoxymethylenemalonate (7.3 g, 34 mmol) as starting materials, the title compound (5.8 g, 78%) was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445509B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-73c5d82c64d0478d9cbfd71b4939f4ba |
| Source note | uspto-grants-2013_05 |