HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (ethoxymethylene)malonate → HCID 58158459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,4-Difluorophenylhydrazine hydrochloride | HCID 2733301 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58158459 | HCID 58158459 | 66.6% |
Reaction Steps
In the same manner as in Reference Example 63 and using (2,4-difluorophenyl)hydrazine•hydrochloride (5.1 g, 28 mmol), water (100 mL), potassium carbonate (8.6 g, 62 mmol) and diethyl ethoxymethylenemalonate (7.4 g, 34 mmol) as starting materials, the title compound (5.0 g, 66%) was obtained as a pale-yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445509B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-3263d2b169034d7395a46cfbdb7acc57 |
| Source note | uspto-grants-2013_05 |