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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2095819Generated: November 1, 2026

Diethyl (ethoxymethylene)malonate → HCID 58158589, compound

https://huagongshe.com/reaction/2095819

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl (ethoxymethylene)malonateHCID 6871—
ReactantPotassium CarbonateHCID 11430—
Reactant2-Methoxyphenylhydrazine HydrochlorideHCID 2849445—
SolventWaterHCID 962—
ProductHCID 58158589HCID 5815858978%

Reaction Steps

In the same manner as in Reference Example 63 and using (2-methoxyphenyl)hydrazine•hydrochloride (5.3 g, 30 mmol), water (100 mL), potassium carbonate (9.1 g, 66 mmol) and diethyl ethoxymethylenemalonate (7.8 g, 36 mmol) as starting materials, the title compound (6.1 g, 78%) was obtained as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08445509B2
Source datasetuspto-grants-2013_05
ORD IDord-7328a6bb9ff0435daecc51b68e24f9a2
Source noteuspto-grants-2013_05