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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2095822Generated: October 31, 2026

Diethyl (ethoxymethylene)malonate → HCID 66968556, compound

https://huagongshe.com/reaction/2095822

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl (ethoxymethylene)malonateHCID 6871—
ReactantPotassium CarbonateHCID 11430—
Reactant(2,6-Dichlorophenyl)hydrazine monohydrochlorideHCID 2723909—
SolventWaterHCID 962—
ProductHCID 66968556HCID 6696855673%

Reaction Steps

In the same manner as in Reference Example 63 and using (2,6-dichlorophenyl)hydrazine•hydrochloride (4.8 g, 23 mmol), water (100 mL), potassium carbonate (6.9 g, 50 mmol) and diethyl ethoxymethylenemalonate (5.9 g, 27 mmol) as starting materials, the title compound (5.0 g, 73%) was obtained as a pale-yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08445509B2
Source datasetuspto-grants-2013_05
ORD IDord-b662c7dad6c543a7a123643c8cb0bd37
Source noteuspto-grants-2013_05