HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (ethoxymethylene)malonate → HCID 66968556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (2,6-Dichlorophenyl)hydrazine monohydrochloride | HCID 2723909 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 66968556 | HCID 66968556 | 73% |
Reaction Steps
In the same manner as in Reference Example 63 and using (2,6-dichlorophenyl)hydrazine•hydrochloride (4.8 g, 23 mmol), water (100 mL), potassium carbonate (6.9 g, 50 mmol) and diethyl ethoxymethylenemalonate (5.9 g, 27 mmol) as starting materials, the title compound (5.0 g, 73%) was obtained as a pale-yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445509B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-b662c7dad6c543a7a123643c8cb0bd37 |
| Source note | uspto-grants-2013_05 |