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HRID2096099

反应详情

EQUATION

反应方程式

HRID 2096099 的结构方程式

REACTANTS

反应物

2
结构：CCOP(OCC)OCC
HCID31215

Triethyl phosphite

C6H15O3P

结构：COc1ccc(CCl)cc1
HCID69993

4-Methyloxybenzyl chloride

C8H9ClO

PRODUCTS

生成物

1
结构：CCOP(=O)(Cc1ccc(OC)cc1)OCC
HCID4063826

Diethyl P-[(4-methoxyphenyl)methyl]phosphonate

C12H19O4P

PROCEDURE

实验过程

4-methoxybenzylchloride and triethyl phosphite were reacted at 150° C. for 5 hours, followed by vacuum distillation for removal of excess triethyl phosphite and by-products to give diethyl 4-methoxybenzylphosphonate.

WORKUP

后处理

  1. distillationfollowed by vacuum distillation for removal of excess triethyl phosphite and by-products