HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → Diethyl P-((4-methoxyphenyl)methyl)phosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Product | Diethyl P-((4-methoxyphenyl)methyl)phosphonate | HCID 4063826 | — |
Reaction Steps
4-methoxybenzylchloride and triethyl phosphite were reacted at 150° C. for 5 hours, followed by vacuum distillation for removal of excess triethyl phosphite and by-products to give diethyl 4-methoxybenzylphosphonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450033B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-987b99d28beb45e1b5b1817e903611ee |
| Source note | uspto-grants-2013_05 |