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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2096993Generated: October 30, 2026

Diethyl Ether → HCID 25222139, compound

https://huagongshe.com/reaction/2096993

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
ReactantBenzylamineHCID 7504—
ReactantTriethylamineHCID 8471—
ReactantHCID 86647220HCID 86647220—
SolventDimethylformamideHCID 6228—
ProductHCID 25222139HCID 25222139—

Reaction Conditions

Temperature20 °C

Reaction Steps

To a solution of 5,7-dinitro-3-iso-propylimidazo[4,5-b]pyridine, 5, in DMF was added NEt3 and benzylamine. After 6 h stirring at 20° C., 15 mL Et2O was added and the solid which precipited was filtered and washed with Et2O.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08450342B2
Source datasetuspto-grants-2013_05
ORD IDord-0d0c2e43d9de4433897f06e7b002a98e
Source noteuspto-grants-2013_05